The development of highly active and long-term stable electrocatalysts for the hydrogen evolution reaction (HER) is very important. Because of the hysteresis phenomenon, IrO2 is rarely used as a cathode material for the HER. Herein, an IrO2-TiO2 composite oxide was prepared using the thermal decomposition method. The physical and electrochemical characterization of the materials was achieved by scanning electron microscopy (SEM), X-ray fluorescence (XRF), X-ray diffraction (XRD), cyclic voltammetry (CV) and electrochemical impedance spectroscop...