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Dispersive micro-solid phase extraction using magnetic ZnFe2O4 nanotubes as adsorbent for preconcentration of Co(II), Ni(II), Mn(II) and Cd(II) followed by ICP-MS determination

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成果类型:
期刊论文
作者:
Chen, Shizhong*;Yan, Juntao;Li, Jianfen;Lu, Dengbo
通讯作者:
Chen, Shizhong
作者机构:
[Chen, Shizhong; Lu, Dengbo] Wuhan Polytech Univ, Coll Food Sci & Engn, Wuhan 430023, Hubei, Peoples R China.
[Li, Jianfen; Yan, Juntao] Wuhan Polytech Univ, Coll Chem & Environm Engn, Wuhan 430023, Hubei, Peoples R China.
通讯机构:
[Chen, Shizhong] W
Wuhan Polytech Univ, Coll Food Sci & Engn, Wuhan 430023, Hubei, Peoples R China.
语种:
英文
关键词:
Cobalt;Nickel;Manganese;Cadmium;Magnetic ZnFe2O4 nanotubes;Dispersive micro-solid phase extraction;Inductively coupled plasma mass spectrometry
期刊:
Microchemical Journal
ISSN:
0026-265X
年:
2019
卷:
147
页码:
232-238
基金类别:
Research and Innovation Initiatives of Wuhan Polytechnic University [2018J04]; Special Fund for Agro-scientific Research in the Public Interest [201503135-2]
机构署名:
本校为第一且通讯机构
院系归属:
食品科学与工程学院
化学与环境工程学院
摘要:
In this work, magnetic ZnFe2O4 nanotubes (ZFONTs) were synthesized, characterized and used as adsorbent for dispersive micro-solid phase extraction of Co(II), Ni(II), Mn(II) and Cd(II) before their determination by inductively coupled plasma mass spectrometry. Adsorption behaviors of target ions on ZFONTs were investigated. The results showed that the analytes were quantitatively retained on ZFONTs in the pH range of 6.0-8.0, and eluted completely with 1.0 mL of 0.4 mol L-1 HNO3. The separation of sorbent from aqueous phase was performed by an external magnet to avoid tedious centrifugation or...

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