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Solidified Floating Organic Drop Microextraction for the Determination of Trace Dy and Y by Electrothermal Vaporization Inductively Coupled Plasma Mass Spectrometry

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成果类型:
期刊论文
作者:
Chen, Shizhong*;Zhu, Shengping;Lu, Dengbo
通讯作者:
Chen, Shizhong
作者机构:
[Chen, Shizhong; Zhu, Shengping; Lu, Dengbo] Wuhan Polytech Univ, Coll Chem & Environm Engn, Wuhan 430023, Peoples R China.
通讯机构:
[Chen, Shizhong] W
Wuhan Polytech Univ, Coll Chem & Environm Engn, Wuhan 430023, Peoples R China.
语种:
英文
关键词:
Solidified Floating;Microextraction;Determination
期刊:
ATOMIC SPECTROSCOPY
ISSN:
0195-5373
年:
2014
卷:
35
期:
1
页码:
1-6
基金类别:
Nature Science Foundation; Education Department Foundation of Hubei Province in China
机构署名:
本校为第一且通讯机构
院系归属:
化学与环境工程学院
摘要:
A method, was developed for the determination of trace Dy and Y in biological and environmentar water samples based on solidified floating organic drop microextraction (SFODME) combined with electrothermal vaporization (ETV) inductively coupled. plasma mass spectrometry (ICP-MS). l-(2-pyridylazo)-2-naphthol (PAN) was used as both chelating reagent in SFODME and chemical modifier in ETV for separation, preconcentration, and volatilization of the REEs prior to their determination. The main factors affecting the preconcentration and determination, including pH, amount of PAN, extraction time, sti...

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