New polyoxomolybdate compounds synthesized in situ using ionic liquid 1-butyl-3-methyl-imidazolium tetrafluoroborate as green solvent

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成果类型：

期刊论文

作者：

Linguito, Stephen L.;Zhang, Xiao;Padmanabhan, Moothetty;Biradar, Ankush V.;Xu, Taotao;...

通讯作者：

Li, Jing

作者机构：

[Zhang, Xiao; Biradar, Ankush V.; Padmanabhan, Moothetty; Asefa, Tewodros; Li, Jing; Emge, Thomas J.; Linguito, Stephen L.] Rutgers State Univ, Dept Chem & Chem Biol, Piscataway, NJ 08854 USA.

[Biradar, Ankush V.; Asefa, Tewodros] Rutgers State Univ, Dept Chem & Biochem Engn, Piscataway, NJ 08854 USA.

[Xu, Taotao] Wuhan Polytech Univ, Elect & Elect Engn Coll, Wuhan 430023, Hubei, Peoples R China.

[Li, Jing] Rutgers State Univ, Dept Chem & Chem Biol, 610 Taylor Rd, Piscataway, NJ 08854 USA.

通讯机构：

[Li, Jing] R

Rutgers State Univ, Dept Chem & Chem Biol, 610 Taylor Rd, Piscataway, NJ 08854 USA.

语种：

英文

关键词：

1 butyl 3 methylimidazolium tetrafluoroborate;acetonitrile;benzaldehyde;hydrogen peroxide;ionic liquid;article;conformation;crystal structure;crystallization;hydrogen bond;oxidation;priority journal;synthesis;thermogravimetry;X ray diffraction

期刊：

NEW JOURNAL OF CHEMISTRY

ISSN：

1144-0546

年：

2013

卷：

期：

页码：

2894-2901

DOI：

10.1039/c3nj00669g

机构署名：

本校为其他机构

院系归属：

电气与电子工程学院

摘要：

Herein we report the facile, green syntheses of three new polyoxomolybdate-based inorganic-organic hybrid materials using room temperature ionic liquid (RTIL), 1-butyl-3-methyl-imidazolium tetrafluoroborate (bmim)[BF4], as a green and reactive solvent. The organic imidazolium component of the RTIL was incorporated into all three structures, the μ5-oxo octamolybdate cluster compound (bmim)3NH 4[Mo8O26] (1) and two Keggin-type cluster compounds, one being a charge transfer salt (bmim)4[PMo VMo11O40] (2) and the other having the unreduced anion (...

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New polyoxomolybdate compounds synthesized in situ using ionic liquid 1-butyl-3-methyl-imidazolium tetrafluoroborate as green solvent

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