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Magnetic ZnFe2O4 nanotubes for dispersive micro solid-phase extraction of trace rare earth elements prior to their determination by ICP-MS

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成果类型:
期刊论文
作者:
Chen, Shizhong*;Yan, Juntao;Li, Jianfen;Lu, Dengbo
通讯作者:
Chen, Shizhong
作者机构:
[Chen, Shizhong; Lu, Dengbo] Wuhan Polytech Univ, Coll Food Sci & Engn, Wuhan 430023, Hubei, Peoples R China.
[Li, Jianfen; Yan, Juntao] Wuhan Polytech Univ, Coll Chem & Environm Engn, Wuhan 430023, Hubei, Peoples R China.
通讯机构:
[Chen, Shizhong] W
Wuhan Polytech Univ, Coll Food Sci & Engn, Wuhan 430023, Hubei, Peoples R China.
语种:
英文
关键词:
Water samples;Tea leaves;Human hair;Magnetic separation;Scanning electron microscopy;X-ray diffractometer
期刊:
Microchimica Acta
ISSN:
0026-3672
年:
2019
卷:
186
期:
4
页码:
228
基金类别:
Research and Innovation Initiatives of Wuhan Polytechnic University#&#&#2018J04 Special Fund for Agro-scientific Research in the Public Interest#&#&#201503135-22
机构署名:
本校为第一且通讯机构
院系归属:
食品科学与工程学院
化学与环境工程学院
摘要:
Magnetic ZnFe2O4 nanotubes (ZFONTs) with numerous pores on their walls were synthesized and characterized. They are shown to be a viable sorbent for dispersive micro-solid phase extraction of the trivalent ions of rare earth elements (REEs), specifically of lanthanum, praseodymium, europium, gadolinium, holmium and ytterbium. The specific surface area of ZFONTs is large (57 m(2)g(-1)) and much bigger than that of ZnFeO4 nanoparticles (16 m(2)g(-1)). It is shown that REEs are quantitatively retained on ZFONTs in the pH range of 7.0-9.0. The separation of the sorbent from the aqueous phase was a...

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