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Magnetic ZnFe 2 O 4 nanotubes for dispersive micro solid-phase extraction of trace rare earth elements prior to their determination by ICP-MS

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成果类型:
期刊论文
作者:
Chen, Shizhong*;Yan, Juntao;Li, Jianfen;Lu, Dengbo
通讯作者:
Chen, Shizhong
作者机构:
[Chen, Shizhong; Lu, Dengbo] Wuhan Polytech Univ, Coll Food Sci & Engn, Wuhan 430023, Hubei, Peoples R China.
[Li, Jianfen; Yan, Juntao] Wuhan Polytech Univ, Coll Chem & Environm Engn, Wuhan 430023, Hubei, Peoples R China.
通讯机构:
[Chen, Shizhong] W
Wuhan Polytech Univ, Coll Food Sci & Engn, Wuhan 430023, Hubei, Peoples R China.
语种:
英文
关键词:
Water samples;Tea leaves;Human hair;Magnetic separation;Scanning electron microscopy;X-ray diffractometer
期刊:
Microchimica Acta
ISSN:
0026-3672
年:
2019
卷:
186
期:
4
页码:
228
基金类别:
Acknowledgments This work was supported by the Research and
机构署名:
本校为第一且通讯机构
院系归属:
食品科学与工程学院
化学与环境工程学院
摘要:
Magnetic ZnFe 2 O 4 nanotubes (ZFONTs) with numerous pores on their walls were synthesized and characterized. They are shown to be a viable sorbent for dispersive micro-solid phase extraction of the trivalent ions of rare earth elements (REEs), specifically of lanthanum, praseodymium, europium, gadolinium, holmium and ytterbium. The specific surface area of ZFONTs is large (57m 2 ⋅g −1 ) and much bigger than that of ZnFeO 4 nanoparticles (16m 2 ⋅g −1 ). It is shown that REEs are quantitatively retained on ZFONTs in the pH range of 7.0–9.0....

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