Cerium dioxide catalyzed synthesis of methyl N-phenylcarbamate from carbon dioxide, aniline and methanol in the presence of n-butyllithium

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成果类型：

期刊论文

作者：

Fan, Guozhi*;Luo, Shanshan;Fang, Tao;Wu, Qiang;Song, Guangsen;...

通讯作者：

Fan, Guozhi

作者机构：

[Li, Jianfen; Song, Guangsen; Fan, Guozhi; Luo, Shanshan; Fang, Tao; Wu, Qiang] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Hubei, Peoples R China.

通讯机构：

[Fan, Guozhi] W

Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Hubei, Peoples R China.

语种：

英文

关键词：

Aniline;Carbon dioxide;CeO2;Methanol;Methyl;N-phenylcarbamate

期刊：

Journal of Molecular Catalysis A: Chemical

ISSN：

1381-1169

年：

2015

卷：

404-405

页码：

92-97

DOI：

10.1016/j.molcata.2015.04.017

基金类别：

Scientific Research Project from Hubei Provincial Department of Education [D20141704]

机构署名：

本校为第一且通讯机构

院系归属：

化学与环境工程学院

摘要：

Direct synthesis of methyl N-phenylcarbamate (MPC) from carbon dioxide (CO<inf>2</inf>), aniline and methanol catalyzed by cerium dioxide (CeO<inf>2</inf>) in the presence of n-butyllithium (BuLi) was developed. The catalytic activity of CeO<inf>2</inf>was significantly improved by the addition of BuLi. The conversion of aniline and the yield of MPC were dependent on the amount of CeO<inf>2</inf>and BuLi, reaction conditions including the pressure of CO<inf>2</inf>, reaction time and temperature, and 9.4% yield of MPC was obtained und...

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Cerium dioxide catalyzed synthesis of methyl N-phenylcarbamate from carbon dioxide, aniline and methanol in the presence of n-butyllithium

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