Determination of N-epsilon-(carboxymethyl)lysine in commercial dairy products in China with liquid chromatography tandem mass spectroscopy

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成果类型：

期刊论文

作者：

Xiao, Shen-Sheng;Shi, Lei;Wang, Peng-Cheng;Liu, Xin;Fang, Min;...

通讯作者：

Gong, Zhi-Yong

作者机构：

[Wu, Yong-Ning; Xiao, Shen-Sheng; Wang, Peng-Cheng; Gong, Zhi-Yong; Liu, Xin; Fang, Min] Wuhan Polytech Univ, Key Lab Deep Proc Major Grain & Oil, Coll Food Sci & Engn, Minist Educ, 68 Univ South Rd, Wuhan 430023, Hubei, Peoples R China.

[Xiao, Shen-Sheng; Wang, Peng-Cheng; Gong, Zhi-Yong; Liu, Xin; Fang, Min] Wuhan Polytech Univ, Hubei Key Lab Proc & Transformat Agr Prod, Coll Food Sci & Engn, Wuhan 430023, Peoples R China.

[Wu, Yong-Ning] China Natl Ctr Food Safety Risk Assessment, Beijing 100022, Peoples R China.

[Shi, Lei] Environm Technol Res Inst Everbright Environm, Qingdao 266033, Peoples R China.

[Shi, Lei] Qingdao Univ Technol, Qingdao 266033, Peoples R China.

通讯机构：

[Gong, Zhi-Yong] W

Wuhan Polytech Univ, Key Lab Deep Proc Major Grain & Oil, Coll Food Sci & Engn, Minist Educ, 68 Univ South Rd, Wuhan 430023, Hubei, Peoples R China.

Wuhan Polytech Univ, Hubei Key Lab Proc & Transformat Agr Prod, Coll Food Sci & Engn, Wuhan 430023, Peoples R China.

语种：

英文

关键词：

Advanced glycation end-product;N-epsilon-(carboxymethyl)lysine (CML);LC-MS/MS;Dairy product;Sterilization;Pasteurization

期刊：

Journal of Food Measurement and Characterization

ISSN：

2193-4126

年：

2022

卷：

期：

页码：

714-721

DOI：

10.1007/s11694-021-01193-1

基金类别：

This study was funded by the Research and Innovation Initiatives of WHPU (2015y13).

机构署名：

本校为第一且通讯机构

院系归属：

食品科学与工程学院

摘要：

A liquid chromatography tandem mass spectroscopy method was employed to determine free and protein-bound Nε-(carboxymethyl)lysine (CML) in seven categories of dairy products (liquid milk n = 28, milk powder n = 26, condensed milk n = 6, milk fats n = 4, cheese n = 9, ice cream n = 6, and whey protein n = 3) commonly consumed in China. Recovery of the analyte based on the isotopic internal standard correction ranged from 104 to 115%, with relative standard deviations of less than 5.13%. The limit of quantification was 0.1 μg/kg. An extremely s...

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Determination of N-epsilon-(carboxymethyl)lysine in commercial dairy products in China with liquid chromatography tandem mass spectroscopy

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