武汉市COD排放环境学习曲线及减排潜力分析
作者:
杨奕;周娅;胡纯;刘骏;梅运军
期刊:
武汉轻工大学学报 ,2019年38(5):55-58 ISSN:2095-7386
作者机构:
武汉轻工大学 化学与环境工程学院,湖北 武汉,430023;[杨奕; 刘骏; 周娅; 胡纯; 梅运军] 武汉轻工大学
关键词:
COD排放;环境学习曲线;减排潜力
摘要:
依据2009—2015年间武汉市COD排放量、GDP、人口等基本数据,对武汉市COD排放的时序特征、人均COD排放量、万元GDP COD排放量进行了分析并建立了武汉市COD排放的环境学习曲线。结果表明武汉市COD排放量、人均COD排放量、万元GDP COD排放量总体呈现下降的趋势,COD排放的环境学习曲线方程为y=0.026x-1.276 9,并得出在"十三五"末武汉市的COD排放量约为13.395万吨。武汉市经济质量整体偏好,但COD减排的压力依然较大。
语种:
中文
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环境监测实践环节评价考核体系的构建与实践
作者:
黄岚;杨明;刘骏;王文清
期刊:
武汉轻工大学学报 ,2019年38(4):99-102+106 ISSN:2095-7386
作者机构:
武汉轻工大学化学与环境工程学院 湖北武汉430023;[杨明; 王文清; 刘骏; 黄岚] 武汉轻工大学
关键词:
环境监测;实践环节;评价体系;构建与实践
摘要:
环境监测实践环节考核评价体系是衡量实践教学质量和学生学习效果的依据,对实践教学具有重要的导向作用。笔者以考核方式多元化、评价主体多样化、强化过程的实践教学评价体系构建原则.构建了制定方案、实施方案、监测报告、汇总答辩为一级指标的实践教学评价体系。
语种:
中文
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成果导向教育理念(OBE)下的环境工程微生物学课程教学改革与实践
作者:
梅运军;黄岚;胡纯;胡文云;张顺喜;...
期刊:
微生物学通报 ,2018年45(3):609-615 ISSN:0253-2654
作者机构:
[梅运军; 黄岚; 胡纯; 胡文云; 张顺喜; 刘骏] 武汉轻工大学化学与环境工程学院, 湖北, 武汉, 430023
关键词:
环境工程微生物学;成果导向教育理念(OBE);课程改革
摘要:
环境工程微生物学是环境类专业的学科基础课,该课程对学生的知识架构以及应用技能的培养起到了重要支撑作用。为了实现该课程定位目标,达到课程的学习预期,我们将成果导向教育理念(Outcomes-based education,OBE)引入到环境工程微生物学课程教学改革实践中,提出在环境工程微生物学课程教学中实施逆向设计、正向实施的原则,即根据课程定位制定环境工程微生物学的预期学习产出,在预期学习产出的基础上优化教学过程,如对教学内容进行取舍,增强环境工程微生物学与其他课程的协调性,在教学实施中强化学生的主体地位,通过教学方法的改革促成预期学习产出,构建合理的学习评价体系。尽管将OBE理念引入到教学实施中取得了一些成效,但该体系的建设还有待于进一步完善。
语种:
中文
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环境生态学课程形成性评价改革探索与实践
作者:
梅运军;黄岚;胡文云;刘骏;胡纯;...
期刊:
商情:教育论坛 ,2018年(40):185,187 ISSN:1673-4041
作者机构:
武汉轻工大学化学与环境工程学院;[刘骏; 黄岚; 胡纯; 胡文云; 梅运军; 张顺喜] 武汉轻工大学
关键词:
环境生态学;教学改革;形成性评价;课程评价
摘要:
课程考核评价体系改革是课程教学改革的重要组成部分,良好的评价体系能促进教学相长.在环境生态学的课程评价体系中笔者经过近几年的改革探索与实践,将形成性评价引入到环境生态学的课程评价体系中,通过改革评价形式、调整评价主体、丰富评价内容等手段取得了良好的教学效果,为进一步加强环境生态学课程改革奠定了良好的基础.
语种:
中文
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“新时期”环境影响评价课程教学内容变化初探
作者:
刘骏
期刊:
武汉轻工大学学报 ,2018年37(3):117-120 ISSN:2095-7386
作者机构:
武汉轻工大学 化学与环境工程学院 湖北 武汉430023;[刘骏] 武汉轻工大学
关键词:
环境影响评价;教学内容;变化
摘要:
笔者总结了近年来我国在环境影响评价制度中的一系列重大变化,包括法律、法规、标准及导则等方面的关键内容调整。提出了在环境影响评价教学内容制定时,应及时准确的将最新政策传递给学生,并且结合其他课程内容,帮助学生理解各项政策变化的来龙去脉,把握国家制度顶层设计思维的主线,从宏观和微观两个方面理解环评工作的内涵。
语种:
中文
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就业导向的环境工程应用型人才培养模式探究
作者:
梅运军;胡纯;杨明;刘骏;张顺喜;...
期刊:
教育现代化 ,2017年4(30):1-2+10 ISSN:2095-8420
作者机构:
武汉轻工大学 化学与环境工程学院,湖北 武汉,430023;[杨明; 张剑; 刘骏; 胡文云; 胡纯; 梅运军; 张顺喜] 武汉轻工大学
关键词:
就业导向;环境工程;应用型人才;培养模式
摘要:
基于就业导向的环境工程人才培养目标,本文从环境工程专业人才培养的能力取向、创新教学模式构建、课程体系设置、评价体系改革以及建立院企、校友联席制度等几方面探讨了创新人才培养模式。
语种:
中文
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基于卓越工程师培养的固体废物处理与处置课程教学模式探索
作者:
周旻;刘骏;侯浩波;刘慧龙;曾建;...
期刊:
武汉轻工大学学报 ,2016年35(1):104-107 ISSN:2095-7386
作者机构:
武汉大学资源与环境科学学院,湖北武汉,430072;武汉大学资源与环境科学学院,湖北武汉430072;武汉轻工大学化学与环境工程学院,湖北武汉430023;[刘慧龙; 侯浩波; 张维昊; 刘骏; 周旻; 曾建] 武汉大学
关键词:
固体废物处理与处置;教学改革;环境工程;卓越工程师
摘要:
秉承课程改革的指导思想,本文研究了卓越工程师培养计划导引下的固体废物处理与处置课程教学模式,从课程的教学模式、知识结构、实践教学体系等方面进行改革,以适应卓越工程师培养的需要;研究了如何提高环境工程专业人才培养质量的教学方法,提出了专业课教学中,加强教学内容改革,教学中增强专业基础课与专业课之间的联系,加强工程能力的培养教学思路。
语种:
中文
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Life Cycle Assessment of Urban Wastewater Treatment
作者:
Wang Mei* ;Yang Ming;Liu Jun;Li Jian-fen
期刊:
Applied Mechanics and Materials ,2014年535:346-349 ISSN:1660-9336
通讯作者:
Wang Mei
作者机构:
[Yang Ming; Li Jian-fen; Wang Mei; Liu Jun] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Hubei, Peoples R China.
通讯机构:
[Wang Mei] W;Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Hubei, Peoples R China.
会议地点:
Hong Kong, PEOPLES R CHINA
会议主办单位:
[Wang Mei;Yang Ming;Liu Jun;Li Jian-fen] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Hubei, Peoples R China.
会议论文集名称:
Applied Mechanics and Materials
关键词:
AHP;Benefits;LCA;Technology;Urban sewage treatment
摘要:
Effect and benefits of a product or service could be analyzed and evaluated by life cycle assessment during the whole life cycle. Urban sewage treatment plants could improve and control urban water pollution escalating, but it also had certain harm to environment. Effect and benefits of urban wastewater treatment plant A and B were analyzed and evaluated, 13 factors were selected, and comprehensive benefits were researched quantificationally using the method of analytic hierarchy process. It found that urban wastewater treatment plant A who applied A/O process had better benefits than urban wastewater treatment plant B who applied BIOLAK process.
语种:
英文
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Synthesis and application of ion-imprinted polymer particles for solid-phase extraction and determination of trace scandium by ICP-MS in different matrices
作者:
Liu, Jin;Yang, Xiaoli;Cheng, Xianzhong* ;Peng, Yuan;Chen, Hongmei
期刊:
ANALYTICAL METHODS ,2013年5(7):1811-1817 ISSN:1759-9660
通讯作者:
Cheng, Xianzhong
作者机构:
[Cheng, Xianzhong; Peng, Yuan; Liu, Jin; Chen, Hongmei] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.;[Yang, Xiaoli] Wuhan Inst Geol & Mineral Resources, Wuhan 430205, Peoples R China.
通讯机构:
[Cheng, Xianzhong] W;Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
摘要:
A novel Sc(iii) ion-imprinted polymers (Sc-IIP) sorbent was prepared by using Sc(iii) ion-8-hydroxyquinoline complex as the template molecule and methacrylic acid, ethylene glycol dimethacrylate (EGDMA) as the functional monomer and cross-linker, respectively. In the present work, a new method using a microcolumn packed with Sc-IIPs as a solid-phase extraction adsorbent was developed for the selective separation and preconcentration of trace amounts of scandium(iii) prior to the determination by inductively coupled plasma mass spectrometry. Various factors influencing the separation and preconcentration of trace scandium, such as pH, sample flow rate and breakthrough volume, elution concentration and volume were investigated in detail. Scandium can be quantitatively retained on the IIPs sorbent at pH 4.0-6.5 from sample volume up to 300 mL and then eluted efficiently with 5 mL 3% HNO3 solution, therefore an enrichment factor of 60 was accomplished. The maximum adsorption capacity of the ion-imprinted and non-imprinted sorbent was 12.8 mg g -1 and 3.5 mg g-1, respectively. Under optimal conditions, the detection limit for scandium was 0.013 ng L-1 in water, 0.46 ng g-1 in geological sample, and the relative standard deviation was 3.2% (n = 11) at the 0.5 μg L-1. The recoveries of Sc in the spiked environmental water samples ranged from 98.0% to 103% with 100 mL of water sample. The proposed method was validated using certified reference materials and applied to the determination of trace scandium in geological samples and environmental water samples with satisfactory results. © 2013 The Royal Society of Chemistry.
语种:
英文
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A modified persimmon powder sorbent for selective separation and determination of trace gold in geological samples by ICP-MS
作者:
Liu, Jin* ;Zou, Dihua;Yang, Xiaoli;Cheng, Xianzhong;Chen, Qian
期刊:
ANALYTICAL METHODS ,2013年5(23):6774-6780 ISSN:1759-9660
通讯作者:
Liu, Jin
作者机构:
[Liu, Jin; Yang, Xiaoli; Zou, Dihua] Wuhan Inst Geol & Mineral Resources, Wuhan 430205, Peoples R China.;[Cheng, Xianzhong; Chen, Qian] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
通讯机构:
[Liu, Jin] W;Wuhan Inst Geol & Mineral Resources, Wuhan 430205, Peoples R China.
摘要:
A novel method that uses chemically modified persimmon powder for solid extraction of Au prior to the determination by inductively coupled plasma-mass spectrometry (ICP-MS) was investigated. Experimental conditions such as acid concentration, sample flow rate and volume, eluent conditions and interfering ions were carefully examined. Gold can be quantitatively adsorbed on the new sorbent from solution of 3% (v/v) aqua regia, and then the trace gold adsorbed on the microcolumn can be effectively eluted with a mixture of 2.0% thiourea and 0.12 mol L-1 HCl. The transition- and heavy-metal ions did not interfere with either the separation/preconcentration or the determination. The maximum adsorption capacity of the sorbent was 25.3 mg g-1. Under optimal conditions, the detection limit for gold was 1.32 ng L-1 in the geological sample, and the relative standard deviation was 0.83% (n = 11) at 1.0 μg L-1. The proposed method was validated by analyzing three certified reference materials and applied to the preconcentration and determination of trace gold in geological samples with satisfactory results. © 2013 The Royal Society of Chemistry.
语种:
英文
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Remove of Congo Red from wastewater by adsorption onto eggshell membrane
作者:
Liu, Jin;Cheng, Xianzhong* ;Qin, Peng;Pan, Mingying
期刊:
Advanced Materials Research ,2012年599:391-394 ISSN:1022-6680
通讯作者:
Cheng, Xianzhong
作者机构:
[Cheng, Xianzhong; Qin, Peng; Liu, Jin; Pan, Mingying] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
通讯机构:
[Cheng, Xianzhong] W;Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
会议名称:
2012 Global Conference on Civil, Structural and Environmental Engineering, GCCSEE 2012 and the 3rd International Symposium on Multi-field Coupling Theory of Rock and Soil Media and Its Applications, MCTRSM 2012
会议时间:
20 October 2012 through 21 October 2012
会议地点:
China Three Gorges Univ, Yichang, PEOPLES R CHINA
会议主办单位:
China Three Gorges Univ
会议论文集名称:
Advanced Materials Research
关键词:
Biomass;Biosorption;Congo red;Eggshell membrane;Removal
摘要:
<jats:p>The performance of native eggshell membrane in removing of Congo Red (CR) from aqueous solution was investigated. The effect of pH, adsorbent concentration, temperature, and contact time were performed by static testing. The maximum biosorption was both observed at pH 7.0 on the eggshell membrane. Optimal adsorption capacity (112.3 mg g<jats:sup>-1</jats:sup>) at initial concentration 10 mg L-1 and rate (99.17%) was obtained at pH 6.8. Characterization of the bio<jats:sup>Superscript text</jats:sup>sorbent eggshell membrane was performed using scanning electron microscope (SEM), and Fourier transform-infrared (FTIR) spectroscopy. The kinetic and equilibrium studies suggest that the adsorption follows Langmuir isotherm model.</jats:p>
语种:
英文
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对“环境化学”课程教学改革的思考
作者:
刘骏;杨明
期刊:
广东化工 ,2012年39(8):187-187,186 ISSN:1007-1865
作者机构:
武汉工业学院化学与环境工程学院,湖北武汉,430023;[杨明; 刘骏] 武汉工业学院
关键词:
环境化学;教学;改革
摘要:
根据环境化学课程的特点,在环境化学教学内容、教学方法及实践教学方面进行了思考。在教学内容上及时补充对环境化学领域新动态的介绍,增加了对重点案例的研究和热点问题的分析;采用板书、多媒体技术相结合的手段进行教学,注重与学生动手能力的培养和激发学生的学习兴趣。
语种:
中文
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模板法制备TiO2/MnO2与TiO2/Mn3O4复合粒子的研究
作者:
刘骏;李代雄
作者机构:
[刘骏; 李代雄] 武汉工业学院化学与环境工程学院
会议名称:
2011 International Conference on Fuzzy Systems and Neural Computing(FSNC 2011)
会议时间:
2011-02-20
会议地点:
Hong Kong,China
关键词:
模板法;复合粒子
摘要:
为了提高纳米Ti O2粒子的光催化性能和吸附性能,采用模板法制备了纳米Ti O2/Mn O2与Ti O2/Mn3O4复合粒子。通过X射线衍射(XRD)和扫描电子显微镜(SEM)对Ti O2/Mn O2与Ti O2/Mn3O4复合粒子进行了表征,并测试了其对茜素红-甲基橙溶液的吸附与光催化降解性能,结果表明Ti O2/Mn O2与Ti O2/Mn3O4复合粒子具有较好的光催化降解和吸附性能。
语种:
中文
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Eggshell Membrane Microcolumn Solid-Phase Extraction and Determination of Trace Gold in Geological Samples by Inductively Coupled Plasma Mass Spectrometry
作者:
Cheng, Xianzhong* ;Liu, Jin;Yang, Xiaoli;Chen, Hongmei;Wang, Yourong
期刊:
ATOMIC SPECTROSCOPY ,2011年32(5):175-181 ISSN:0195-5373
通讯作者:
Cheng, Xianzhong
作者机构:
[Cheng, Xianzhong; Wang, Yourong; Liu, Jin; Chen, Hongmei] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.;[Yang, Xiaoli] Wuhan Inst Geol & Mineral Resources, Wuhan 430205, Peoples R China.
通讯机构:
[Cheng, Xianzhong] W;Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
摘要:
A chicken eggshell membrane (ESM) was used as a solid-phase extraction adsorbent for the separation and preconcentration in combination with inductively coupled plasma-mass spectrometry (ICP-MS) for the determination of trace gold in geological samples. Gold (Au) was quantitatively separated and preconcentratcd in 1.2 mol L-1 HC1 at a sample flow rate of 2.0 mL min.1 using the ESM microcolumn system. The gold adsorbed on the microcolumn was effectively eluted with a mixture of 1% thiourea and 0.12 mol L1 HCL The effects of acid concentration, sample flow rate and volume, eluent conditions and interfering ions were carefully investigated. The transition- and heavy-metal ions did not interfere with either the separation/preconcentration or the determination. The limit of detection of the method for Au was 0.92 ng L-1. The method was validated using certified reference materials and applied to the determination of trace Au in geological samples with satisfactory results.
语种:
英文
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魔芋粉模板法制备纳米硒
作者:
王文清;刘骏
期刊:
化学世界 ,2011年52(12):720-721,750 ISSN:0367-6358
作者机构:
[王文清; 刘骏] 武汉工业学院化学与环境工程学院
关键词:
魔芋粉;亚硒酸钠;纳米硒
摘要:
以魔芋粉作为软模板,用还原法制备了球状的硒纳米粒子。研究了不同的还原剂、模板剂用量和温度对硒纳米粒子的影响。采用扫描电镜和X射线衍射对产物进行了表征。结果表明,当n(Vc):n(Na_2SeO_3)=3:1、魔芋粉质量分数为3.0×10~(-3)、40℃反应1.5 h时,可得到均匀稳定的球形硒纳米颗粒,平均粒径约60~150 nm。
语种:
中文
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Determination of trace rotenone by UV-Vis spectrophotometry using molecularly imprinted polymer microspheres
作者:
Yang, Ming* ;Chen, Yuantao;Liu, Jun;Ma, Jing;Huai, Lufeng
期刊:
Journal of Analytical Chemistry ,2011年66(9):820-823 ISSN:1061-9348
通讯作者:
Yang, Ming
作者机构:
[Ma, Jing; Huai, Lufeng; Yang, Ming; Liu, Jun] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.;[Chen, Yuantao] Qinghai Normal Univ, Dept Chem, Xining 810008, Peoples R China.
通讯机构:
[Yang, Ming] W;Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
关键词:
Absorbances;Detection limits;Experimental conditions;Molecularly Imprinted Polymer;Optimum conditions;Pre-concentration;Relative standard deviations;rotenone;UV-vis spectrophotometry;UV-visible spectrophotometry;Water samples;Microspheres;Polymers;Spectrophotometry;Trace analysis
摘要:
Novel molecularly imprinted polymer microspheres for rotenone were synthesized. It is capable to adsorb rotenone from aqueous solutions. Combined with the molecularly imprinted polymer micro-spheres, conventional UV-visible spectrophotometry can be effective in determination of rotenone. The experimental conditions were discussed. Under optimum conditions, it was found that the peak of rotenone absorbance is at 298 nm. Rotenone can be determined in the range of 1-200 μg/L, the detection limit for rotenone is 0.5 μg/L. The relative standard deviation for determination of 20 μg/L of rotenone was 2.8%. The method was applied to the determination of rotenone in water samples with satisfactory results. © 2011 Pleiades Publishing, Ltd.
语种:
英文
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Synthesis of TiO2/MnO2 and TiO2/Mn3O4 by Template Method
作者:
Liu Jun* ;Li Dai-xiong
作者机构:
[Liu Jun; Li Dai-xiong] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan, Hubei, Peoples R China.
会议名称:
AASRI Conference on Artificial Intelligence and Industry Application (AASRI-AIIA 2011)
会议时间:
MAY 23-24, 2011
会议地点:
Male, MALDIVES
会议主办单位:
[Liu Jun;Li Dai-xiong] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan, Hubei, Peoples R China.
关键词:
template method;TiO2;Mn3O4;MnO2;composite particle
摘要:
To improve the photocatalysis and absorbability of nanometer TiO2 particles, TiO2/MnO2 and TiO2/Mn3O4 composite particles in micrometer were prepared by template method. The morphologies and structure of the composite particles were characterized by SEM and XRD. The photocatalytic abilities and absorbability of alizarin red and methyl orange solution have been tested. The results show that the composite particles have excellent photocatalytic abilities and absorbability.
语种:
中文
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教学研究型大学实验平台的整合
作者:
王文清;杨明;刘骏
期刊:
广东化工 ,2010年37(7):147-148+153 ISSN:1007-1865
作者机构:
武汉工业学院,化环学院,湖北,武汉,430023;[杨明; 刘骏; 王文清] 武汉工业学院
关键词:
教研型大学;实验平台;整合
摘要:
针对教学研究型大学实验平台整合中存在的管理体制不顺、运行机制不灵、信息传递不畅等问题,根据教研型大学的要求,探讨了"布局合理、理顺体制、资源共享、学科融合、特色突出、科学研究、提高效益"的整合理念和原则,构架了平台整合的模型,提出了"领导重视,分步实施;改革创新,加强实验;以人为本,强化功能;利用网络,实现集成"的整合措施,构建了平台整合后的管理体制.
语种:
中文
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Hydrogen-rich gas production by air–steam gasification of rice husk using supported nano-NiO/γ-Al2O3 catalyst
作者:
Li, Jianfen* ;Liu, Jianjun;Liao, Shiyan;Yan, Rong
期刊:
International Journal of Hydrogen Energy ,2010年35(14):7399-7404 ISSN:0360-3199
通讯作者:
Li, Jianfen
作者机构:
[Li, Jianfen; Liu, Jianjun; Liao, Shiyan; Yan, Rong] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.;[Yan, Rong] Nanyang Technol Univ, Inst Environm Sci & Engn, Singapore 637723, Singapore.
通讯机构:
[Li, Jianfen] W;Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
关键词:
Biomass ratio;Catalytic gasification;Catalytic reactor;Complex effects;Equivalence ratios;Fixed bed reactor;Gas quality;Gas yields;Gasification process;High activity;Higher temperatures;Hydrogen-rich gas;Optimal values;Optimum operating conditions;Rice husk;Steam gasification;Aluminum;Catalyst activity;Catalytic cracking;Chemical reactors;Gas generators;Gas pipelines;Gas producers;Gases;Gasification;Hydrocarbons;Steam;Hydrogen production
摘要:
The air-steam catalytic gasification of rice husk for hydrogen-rich gas production was experimentally investigated in a combined fixed bed reactor with the newly developed nano-NiO/γ-Al2O3 catalyst. A series of experiments have been performed to explore the effects of catalyst presence, catalytic reactor temperature, the equivalence ratio (ER), and steam to biomass ratio (S/B) on the composition and yield of gasification gases. The experiments demonstrated that the developed nano-NiO/γ-Al2O3 catalyst had a high activity of cracking tar and hydrocarbons, upgrading the gas quality, as well as yielding a high hydrogen production. Catalytic temperature was crucial for the overall gasification process, a higher temperature contributed to more hydrogen production and gas yield. Varying ER demonstrated complex effects on rice husk gasification and an optimal value of 0.22 was found in the present study. Compared with biomass catalytic gasification under air only, the introduction of steam improved the gas quality and yield. The steam/biomass ratio of 1.33 was found as the optimum operating condition in the air-steam catalytic gasification. © 2010 Professor T. Nejat Veziroglu.
语种:
英文
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Molecularly imprinted solid-phase extraction for chlorpyrifos determination in water samples
作者:
Liu, Jun* ;Yang, Ming;Huai, Lu Feng
期刊:
Advanced Materials Research ,2010年113-116(229):947-951 ISSN:1022-6680
通讯作者:
Liu, Jun
作者机构:
[Huai, Lu Feng; Yang, Ming; Liu, Jun] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
通讯机构:
[Liu, Jun] W;Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
会议名称:
2010 International Conference of Environment Materials and Environment Management(2010年环境材料与环境管理国际学术会议 EMEM 2010)
会议时间:
2010-07-24
会议地点:
哈尔滨
会议主办单位:
[Liu, Jun;Yang, Ming;Huai, Lu Feng] Wuhan Polytech Univ, Sch Chem & Environm Engn, Wuhan 430023, Peoples R China.
会议论文集名称:
2010 International Conference of Environment Materials and Environment Management(2010年环境材料与环境管理国际学术会议 EMEM 2010)论文集
关键词:
molecularly imprinted polymers;solid-phase extraction;chlorpyrifos
摘要:
The determination of chlorpyrifos at low ngL-1 levels in wastewater requires highly selective and sensitive analytical procedures. The removal of matrix components during sample preparation results in significant benefits towards reducing the matrix effects during GC analysis. Therefore this work describes a simple method to enrich and clean up chlorpyrifos from sewage water using molecularly imprinted solid phase extraction (MISPE). Final analysis was performed by gas chromatography. The performance of this method has been evaluated in water samples in terms of recovery, precision, and method quantification limit. Recovery for chlorpyrifos ranged between 99 and 105% with RSD values below 7.9%. The performance of the method was further emphasized by the study of different water samples. In these samples, chlorpyrifos were detected in concentration above method quantification limits ranging from 50 to 3000 ngL-1. © (2010) Trans Tech Publications, Switzerland.
语种:
英文
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